Graphics

Graphics

Pattern List

Ref.Code     Chem. Formula         Score    Scale Fac.  Mineral Name          
04-012-0489  Ca ( C O3 )                68       0.655  Calcite               
01-070-3755  Si O2                      60       0.316  Quartz                
04-007-2613  Fe S2                      45       0.055  Pyrite                
04-017-1391  Ca Mg0.46 Fe0.54 (..       36       0.046  dolomite              
04-017-0520  K0.7 Na0.01 Ca0.01..       22       0.131  Illite                
04-011-6587  Mg1.3 Fe3.4 Al2.6 ..        4       0.079  Chamosite             

Peak List

Pos.[°2Th.]  d-spacing [Å]  Rel. Int. [%]  Matched by
     8.8287       10.01620           2.37  04-017-0520       
    12.5263        7.06666           6.12  04-011-6587       
    17.8320        4.97423           0.50                    
    19.7743        4.48981           2.23  04-017-0520       
    20.8649        4.25752           7.50  01-070-3755       
    23.0891        3.85218           9.78  04-012-0489;04..  
    23.9844        3.71039           1.12  04-017-1391       
    25.2195        3.53140           2.64  04-011-6587       
    26.6546        3.34443          35.62  01-070-3755;04..  
    28.5147        3.13036           1.47  04-007-2613;04..  
    29.4466        3.03337         100.00  04-012-0489       
    30.8365        2.89975           5.60  04-017-1391       
    31.4763        2.84226           2.14  04-012-0489;04..  
    33.0501        2.71042           5.70  04-007-2613       
    34.6147        2.58926           0.78  04-017-0520       
    34.9730        2.56568           1.81  04-017-0520       
    36.0039        2.49454          10.19  04-012-0489       
    36.5532        2.45831           2.71  01-070-3755;04..  
    37.0645        2.42556           2.22  04-007-2613;04..  
    37.6216        2.38894           0.80  04-017-0520       
    37.8205        2.37683           0.62  04-017-0520       
    39.4607        2.28362          17.05  04-012-0489;01..  
    40.2691        2.23962           0.70  01-070-3755;04..  
    40.7561        2.21398           2.15  04-007-2613;04..  
    41.0146        2.19880           1.04  04-017-1391;04..  
    42.4214        2.13085           1.72  01-070-3755;04..  
    43.2132        2.09362          12.64  04-012-0489;04..  
    44.7964        2.02324           1.07  04-017-1391;04..  
    45.7823        1.98194           1.30  01-070-3755;04..  
    47.1785        1.92649           4.28  04-012-0489;04..  
    47.5786        1.91122          15.24  04-012-0489       
    48.5610        1.87483          13.14  04-012-0489;04..  
    50.1267        1.81988           3.77  01-070-3755;04..  
    50.9754        1.79155           0.64  04-017-1391;04..  
    54.8627        1.67346           0.88  01-070-3755;04..  
    56.2748        1.63477           2.26  04-007-2613;04..  
    56.6266        1.62545           1.92  04-012-0489       
    57.4828        1.60326           4.62  04-012-0489;04..  
    58.2050        1.58507           0.42  04-012-0489;04..  
    59.6190        1.54953           0.78  04-017-1391;04..  
    59.9488        1.54307           2.38  01-070-3755       
    60.7501        1.52462           3.18  04-012-0489;04..  
    61.1283        1.51484           1.85  04-012-0489;04..  
    61.6465        1.50459           1.89  04-007-2613;04..  
    63.2229        1.47082           0.94  04-012-0489;04..  
    64.2316        1.45013           1.13  04-007-2613;04..  
    64.7485        1.43980           3.14  04-012-0489;04..  
    65.6920        1.42139           1.90  04-012-0489;01..  
    67.7112        1.38383           1.03  01-070-3755;04..  
    68.1291        1.37636           1.64  01-070-3755;04..  
    68.3085        1.37205           1.47  01-070-3755;04..  
    69.3401        1.35526           0.38  04-012-0489;04..  

Anchor Scan Parameters

Dataset Name:	MT 16
File name:	C:\XRD Data\MT 16.xrdml
Comment:	Configuration=Spinner Srage - Transmission, Owner=User-1, Creation date=11/5/2013 2:01:36 PM
	Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
	Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size Phi:0.1
	Diffractometer system=XPERT-PRO
	Measurement program=C:\Users\SEMCAL_XRD\Documents\Marcellus MSEEL\MT 16.xrdmp, Identifier={21B0662C-6956-4B26-8D20-669EBF78BF81}
	Batch program=C:\PANalytical\Data Collector\Programs\Xcelerator batch.xrdmp, Identifier={15A30A00-6FD7-42F1-923A-CC77284190FA}
	MT 16
Measurement Date / Time:	6/14/2016 5:19:17 PM
Operator:	SEMCAL_XRD
Raw Data Origin:	XRD measurement (*.XRDML)
Scan Axis:	Gonio
Start Position [°2Th.]:	5.0084
End Position [°2Th.]:	69.9824
Step Size [°2Th.]:	0.0170
Scan Step Time [s]:	20.3200
Scan Type:	Continuous
PSD Mode:	Scanning
PSD Length [°2Th.]:	2.12
Offset [°2Th.]:	0.0000
Divergence Slit Type:	Fixed
Divergence Slit Size [°]:	0.2177
Specimen Length [mm]:	10.00
Measurement Temperature [°C]:	25.00
Anode Material:	Cu
K-Alpha1 [Å]:	1.54060
K-Alpha2 [Å]:	1.54443
K-Beta [Å]:	1.39225
K-A2 / K-A1 Ratio:	0.50000
Generator Settings:	40 mA, 45 kV
Diffractometer Type:	0000000011117966
Diffractometer Number:	0
Goniometer Radius [mm]:	240.00
Dist. Focus-Diverg. Slit [mm]:	100.00
Incident Beam Monochromator:	No
Spinning:	Yes

Document History

Insert Measurement:
- File name = "MT 16.xrdml"
- Modification time = "10/4/2017 2:55:23 PM"
- Modification editor = "SEMCAL_XRD"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "10/4/2017 2:55:23 PM"
- Modification editor = "SEMCAL_XRD"

Interpolate Step Size:
- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "10/4/2017 2:55:23 PM"
- Modification editor = "PANalytical"

Determine Background:
- Add to net scan = "Nothing"
- User defined intensity = "-5"
- Correction method = "Automatic"
- Bending factor = "2"
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "No"
- Granularity = "20"
- Modification time = "10/4/2017 1:21:36 PM"
- Modification editor = "SEMCAL_XRD"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "4/28/2017 4:58:53 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "34.6147"
- Modification time = "10/4/2017 2:57:04 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "37.6216"
- Modification time = "10/4/2017 2:57:08 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "37.8205"
- Modification time = "10/4/2017 2:57:11 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "41.0146"
- Modification time = "10/4/2017 2:57:14 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "59.6190"
- Modification time = "10/4/2017 2:57:32 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "61.1283"
- Modification time = "10/4/2017 2:57:44 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "68.3085"
- Modification time = "10/4/2017 2:58:01 PM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "10/4/2017 2:58:32 PM"
- Modification editor = "SEMCAL_XRD"