Graphics

Graphics

Pattern List

Ref.Code     Chem. Formula         Score    Scale Fac.  Mineral Name          
01-070-3755  Si O2                      62       0.687  Quartz                
04-012-0489  Ca ( C O3 )                58       0.392  Calcite               
04-011-6849  K Al2 Si4 O10 ( O ..       38       0.234  Muscovite-2M1         
04-015-9853  Ca Mg ( C O3 )2            23       0.036  dolomite              
00-006-0710  Fe S2                      15       0.017  Pyrite, syn           
00-003-0508  Na Al Si3 O8               11       0.050  Albite                
01-085-2163  ( Mg5.036 Fe4.964 ..       24       0.055  Chamosite-1MIIb       

Peak List

Pos.[°2Th.]  d-spacing [Å]  Rel. Int. [%]  Matched by
     6.2579       14.12413           2.86  01-085-2163       
     8.8555        9.98598          13.25  04-011-6849       
    12.5481        7.05445           9.05  01-085-2163       
    17.7427        4.99907           3.45  04-011-6849       
    18.8405        4.71018           1.19  01-085-2163       
    19.8711        4.46816           6.78  04-011-6849       
    20.8720        4.25609          21.22  01-070-3755;04..  
    22.0738        4.02702           0.71  04-015-9853       
    23.0993        3.85051           6.63  04-012-0489       
    23.8159        3.73624           1.79  04-011-6849       
    24.3271        3.65888           0.81  00-003-0508       
    25.2160        3.53189           4.51  01-085-2163       
    25.4908        3.49443           2.58  04-011-6849;01..  
    26.6579        3.34402         100.00  01-070-3755;04..  
    27.7592        3.21381           2.48  04-011-6849       
    27.9392        3.19351           3.78  04-011-6849;00..  
    29.4527        3.03276          67.96  04-012-0489       
    29.8690        2.98896           3.60  04-011-6849       
    30.8495        2.89856           3.35  04-015-9853;00..  
    31.2370        2.86111           2.25  04-011-6849       
    31.5412        2.83420           1.92  04-012-0489;01..  
    31.9876        2.79798           1.47  04-011-6849       
    33.0373        2.71144           1.66  00-006-0710       
    34.5391        2.59691           3.09  04-011-6849       
    34.6862        2.58409           3.15  04-011-6849       
    34.9940        2.56418           7.09  04-011-6849;01..  
    36.0461        2.49172           8.59  04-012-0489;04..  
    36.5490        2.45858           8.83  01-070-3755;04..  
    37.0317        2.42563           1.00  00-006-0710;01..  
    37.4720        2.39813           1.90  04-011-6849;04..  
    37.7706        2.38183           2.05  04-011-6849       
    39.4766        2.28274          16.74  01-070-3755;04..  
    40.2864        2.23870           3.59  01-070-3755;04..  
    41.0365        2.19950           1.13  04-011-6849;04..  
    42.0204        2.14847           1.28  04-011-6849       
    42.4381        2.13005           6.18  01-070-3755;04..  
    43.2334        2.09269           8.50  04-012-0489;00..  
    44.9373        2.01555           0.85  04-015-9853;01..  
    45.3303        2.00064           2.16  04-011-6849;01..  
    45.7834        1.98189           3.13  01-070-3755;04..  
    47.1875        1.92614           3.01  04-012-0489;04..  
    47.6036        1.91027           9.50  04-012-0489       
    48.5451        1.87541           7.51  04-012-0489;04..  
    50.1243        1.81996          10.91  01-070-3755;04..  
    54.8578        1.67359           2.83  01-070-3755;04..  
    55.3114        1.66094           1.85  01-070-3755;04..  
    55.7574        1.64734           0.75  04-011-6849;00..  
    56.2697        1.63355           0.81  04-011-6849;00..  
    56.6490        1.62486           1.39  04-012-0489;04..  
    57.4415        1.60431           2.98  04-012-0489;04..  
    59.5952        1.55009           0.72  04-011-6849;01..  
    59.9422        1.54322           7.28  01-070-3755;04..  
    60.7547        1.52452           2.32  04-012-0489;04..  
    61.7249        1.50286           2.91  04-011-6849;00..  
    63.1701        1.47192           0.77  04-012-0489;04..  
    64.0205        1.45440           1.33  01-070-3755;04..  
    64.7698        1.43938           1.99  04-012-0489;04..  
    65.6430        1.42115           0.89  01-070-3755;04..  
    65.7932        1.41945           1.55  01-070-3755;04..  
    67.7337        1.38343           4.26  01-070-3755;01..  
    68.1296        1.37635           5.19  01-070-3755;04..  
    69.4214        1.35275           0.81  04-011-6849       

Anchor Scan Parameters

Dataset Name:	TL 36
File name:	C:\XRD Data\TL 36.xrdml
Comment:	Configuration=Spinner Srage - Transmission, Owner=User-1, Creation date=11/5/2013 2:01:36 PM
	Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
	Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size Phi:0.1
	Diffractometer system=XPERT-PRO
	Measurement program=C:\Users\SEMCAL_XRD\Documents\Marcellus MSEEL\TL 36.xrdmp, Identifier={17030176-2244-482E-B7BF-3167740379E1}
	Batch program=C:\PANalytical\Data Collector\Programs\Xcelerator batch.xrdmp, Identifier={648876B1-55CE-4EB3-BCAA-2428E7DBD6EC}
	TL 36
Measurement Date / Time:	7/1/2016 4:22:46 PM
Operator:	SEMCAL_XRD
Raw Data Origin:	XRD measurement (*.XRDML)
Scan Axis:	Gonio
Start Position [°2Th.]:	5.0084
End Position [°2Th.]:	69.9824
Step Size [°2Th.]:	0.0170
Scan Step Time [s]:	20.3200
Scan Type:	Continuous
PSD Mode:	Scanning
PSD Length [°2Th.]:	2.12
Offset [°2Th.]:	0.0000
Divergence Slit Type:	Fixed
Divergence Slit Size [°]:	0.2177
Specimen Length [mm]:	10.00
Measurement Temperature [°C]:	25.00
Anode Material:	Cu
K-Alpha1 [Å]:	1.54060
K-Alpha2 [Å]:	1.54443
K-Beta [Å]:	1.39225
K-A2 / K-A1 Ratio:	0.50000
Generator Settings:	40 mA, 45 kV
Diffractometer Type:	0000000011117966
Diffractometer Number:	0
Goniometer Radius [mm]:	240.00
Dist. Focus-Diverg. Slit [mm]:	100.00
Incident Beam Monochromator:	No
Spinning:	Yes

Document History

Insert Measurement:
- File name = "TL 36.xrdml"
- Modification time = "9/20/2016 11:15:00 AM"
- Modification editor = "SEMCAL_XRD"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "9/20/2016 11:15:00 AM"
- Modification editor = "SEMCAL_XRD"

Interpolate Step Size:
- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "9/20/2016 11:15:00 AM"
- Modification editor = "PANalytical"

Determine Background:
- Add to net scan = "Nothing"
- User defined intensity = "-5"
- Correction method = "Automatic"
- Bending factor = "2"
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "Yes"
- Granularity = "20"
- Modification time = "9/19/2016 2:51:36 PM"
- Modification editor = "SEMCAL_XRD"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "8/18/2016 10:13:32 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "31.5412"
- Modification time = "9/20/2016 11:21:30 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "31.2370"
- Modification time = "9/20/2016 11:21:34 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "29.8690"
- Modification time = "9/20/2016 11:21:41 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "34.6862"
- Modification time = "9/20/2016 11:21:49 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "37.0317"
- Modification time = "9/20/2016 11:21:53 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "37.4720"
- Modification time = "9/20/2016 11:21:58 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "42.0204"
- Modification time = "9/20/2016 11:22:11 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "44.9373"
- Modification time = "9/20/2016 11:22:18 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "55.7574"
- Modification time = "9/20/2016 11:22:23 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "56.2697"
- Modification time = "9/20/2016 11:22:24 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "59.5952"
- Modification time = "9/20/2016 11:22:30 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "65.6430"
- Modification time = "9/20/2016 11:22:41 AM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "69.4214"
- Modification time = "9/20/2016 11:22:55 AM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "9/20/2016 11:23:30 AM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "9/20/2016 11:24:55 AM"
- Modification editor = "SEMCAL_XRD"