Graphics

Graphics

Pattern List

Ref.Code     Chem. Formula         Score    Scale Fac.  Mineral Name          
04-012-0489  Ca ( C O3 )                67       0.782  Calcite               
01-070-3755  Si O2                      58       0.043  Quartz                
00-036-0426  Ca Mg ( C O3 )2            12       0.006  Dolomite              
00-001-1295  Fe S2                 Unmatch       0.163  Pyrite                

Peak List

Pos.[°2Th.]  d-spacing [Å]  Rel. Int. [%]  Matched by
    20.8598        4.25856           1.21  01-070-3755       
    23.0756        3.85441           4.63  04-012-0489       
    26.6487        3.34516           4.45  01-070-3755       
    28.4888        3.13314           0.29  00-001-1295       
    29.4432        3.03372         100.00  04-012-0489       
    30.9938        2.88539           1.16  00-036-0426       
    31.4742        2.84244           1.93  04-012-0489       
    33.0604        2.70960           0.10  00-001-1295       
    36.0023        2.49465           4.54  04-012-0489       
    36.5110        2.46105           0.29  01-070-3755       
    39.4322        2.28520           7.96  04-012-0489;01..  
    40.3128        2.23730           0.09  01-070-3755       
    42.4205        2.13089           0.18  01-070-3755       
    43.1819        2.09506           6.78  04-012-0489       
    45.8753        1.97814           0.06  01-070-3755       
    47.1365        1.92811           2.07  04-012-0489       
    47.5377        1.91277          10.77  04-012-0489;00..  
    48.5398        1.87560           8.74  04-012-0489       
    50.1186        1.82015           0.47  01-070-3755       
    54.9029        1.67233           0.06  01-070-3755       
    56.5914        1.62503           1.15  04-012-0489       
    56.7775        1.62417           0.54                    
    57.4297        1.60328           3.16  04-012-0489       
    58.1243        1.58577           0.53  04-012-0489       
    59.9239        1.54237           0.20  01-070-3755;00..  
    60.7136        1.52419           1.83  04-012-0489       
    61.0501        1.51659           1.51  04-012-0489       
    61.4177        1.50839           0.98  04-012-0489       
    63.0891        1.47239           0.62  04-012-0489       
    64.7005        1.43956           1.82  04-012-0489       
    64.8998        1.43919           0.93                    
    65.6583        1.42086           1.81  04-012-0489;01..  
    65.8773        1.42019           1.03                    
    67.6871        1.38312           0.15  01-070-3755       
    68.1173        1.37543           0.20  01-070-3755       
    69.2245        1.35611           0.36  04-012-0489       

Anchor Scan Parameters

Dataset Name:	OL 5
File name:	C:\XRD Data\OL 5.xrdml
Comment:	Configuration=Spinner Srage - Transmission, Owner=User-1, Creation date=11/5/2013 2:01:36 PM
	Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
	Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size Phi:0.1
	Diffractometer system=XPERT-PRO
	Measurement program=C:\Users\SEMCAL_XRD\Documents\Marcellus MSEEL\OL 5.xrdmp, Identifier={A474A703-047F-4306-B60E-193C07F9A2AA}
	Batch program=C:\PANalytical\Data Collector\Programs\Xcelerator batch.xrdmp, Identifier={9398BD5A-F2D4-40EC-8DA0-551CDA476CF2}
	OL 5
Measurement Date / Time:	6/16/2016 4:37:18 PM
Operator:	SEMCAL_XRD
Raw Data Origin:	XRD measurement (*.XRDML)
Scan Axis:	Gonio
Start Position [°2Th.]:	5.0084
End Position [°2Th.]:	69.9824
Step Size [°2Th.]:	0.0170
Scan Step Time [s]:	20.3200
Scan Type:	Continuous
PSD Mode:	Scanning
PSD Length [°2Th.]:	2.12
Offset [°2Th.]:	0.0000
Divergence Slit Type:	Fixed
Divergence Slit Size [°]:	0.2177
Specimen Length [mm]:	10.00
Measurement Temperature [°C]:	25.00
Anode Material:	Cu
K-Alpha1 [Å]:	1.54060
K-Alpha2 [Å]:	1.54443
K-Beta [Å]:	1.39225
K-A2 / K-A1 Ratio:	0.50000
Generator Settings:	40 mA, 45 kV
Diffractometer Type:	0000000011117966
Diffractometer Number:	0
Goniometer Radius [mm]:	240.00
Dist. Focus-Diverg. Slit [mm]:	100.00
Incident Beam Monochromator:	No
Spinning:	Yes

Document History

Insert Measurement:
- File name = "OL 5.xrdml"
- Modification time = "10/4/2017 4:40:51 PM"
- Modification editor = "SEMCAL_XRD"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "10/4/2017 4:40:51 PM"
- Modification editor = "SEMCAL_XRD"

Interpolate Step Size:
- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "10/4/2017 4:40:51 PM"
- Modification editor = "PANalytical"

Determine Background:
- Add to net scan = "Nothing"
- User defined intensity = "-5"
- Correction method = "Automatic"
- Bending factor = "2"
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "No"
- Granularity = "20"
- Modification time = "10/4/2017 1:21:36 PM"
- Modification editor = "SEMCAL_XRD"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "4/28/2017 4:58:53 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "67.6871"
- Modification time = "10/4/2017 4:41:45 PM"
- Modification editor = "SEMCAL_XRD"

Delete Peak(s):
- Start position = "5.1605"
- End position = "5.1605"
- Modification time = "10/4/2017 4:42:09 PM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "10/4/2017 4:42:28 PM"
- Modification editor = "SEMCAL_XRD"