Graphics

Graphics

Pattern List

Ref.Code     Chem. Formula         Score    Scale Fac.  Mineral Name          
04-012-0489  Ca ( C O3 )                69       0.675  Calcite               
01-070-3755  Si O2                      69       0.435  Quartz                
04-004-6511  Fe S2                      48       0.020  Pyrite, syn           
04-015-9850  Ca Mg ( C O3 )2            13       0.011  dolomite              

Peak List

Pos.[°2Th.]  d-spacing [Å]  Rel. Int. [%]  Matched by
    20.8533        4.25988           9.73  01-070-3755       
    23.0859        3.85271           6.35  04-012-0489       
    26.6449        3.34563          48.35  01-070-3755       
    28.4944        3.13254           0.66  04-004-6511       
    29.4556        3.03247         100.00  04-012-0489       
    30.9455        2.88979           1.01  04-015-9850       
    31.5117        2.83914           2.24  04-012-0489       
    33.0567        2.70989           1.75  04-004-6511       
    36.0180        2.49360           7.75  04-012-0489       
    36.5386        2.45926           3.03  01-070-3755       
    37.0942        2.42369           0.72  04-004-6511       
    39.4558        2.28390          13.87  04-012-0489;01..  
    40.2793        2.23908           1.17  01-070-3755       
    40.7501        2.21430           0.60  04-004-6511       
    42.4227        2.13078           2.09  01-070-3755       
    43.2037        2.09406           9.78  04-012-0489       
    45.7756        1.98221           1.16  01-070-3755       
    47.1581        1.92727           3.11  04-012-0489       
    47.5449        1.91250          10.65  04-012-0489;04..  
    48.5476        1.87532           9.98  04-012-0489       
    50.1096        1.82046           4.97  01-070-3755       
    51.0713        1.78842           0.17  04-015-9850       
    54.8439        1.67398           1.31  01-070-3755       
    55.3812        1.65901           0.35  01-070-3755       
    56.2622        1.63511           1.07  04-004-6511       
    56.6174        1.62569           1.67  04-012-0489       
    57.4436        1.60426           3.74  04-012-0489       
    58.1422        1.58663           0.60  04-012-0489       
    59.0698        1.56391           0.15  04-004-6511;04..  
    59.9198        1.54375           2.97  01-070-3755;04..  
    60.7221        1.52526           2.36  04-012-0489       
    61.0717        1.51610           1.25  04-012-0489       
    61.4654        1.50858           1.18  04-012-0489       
    63.1252        1.47286           0.65  04-012-0489       
    64.0041        1.45474           0.49  01-070-3755       
    64.2336        1.44889           0.32  04-004-6511       
    64.7296        1.44017           2.42  04-012-0489       
    65.7114        1.41984           1.80  04-012-0489;01..  
    65.9293        1.41919           1.26                    
    67.7003        1.38289           1.55  01-070-3755;04..  
    68.2022        1.37393           1.95  01-070-3755       
    69.2898        1.35499           0.46  04-012-0489;04..  

Anchor Scan Parameters

Dataset Name:	MO 1
File name:	C:\XRD Data\MO 1.xrdml
Comment:	Configuration=Spinner Srage - Transmission, Owner=User-1, Creation date=11/5/2013 2:01:36 PM
	Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001; Minimum step size Omega:0.001
	Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size Phi:0.1
	Diffractometer system=XPERT-PRO
	Measurement program=C:\Users\SEMCAL_XRD\Documents\Marcellus MSEEL\MO 1.xrdmp, Identifier={25834F23-B353-4600-A8E2-BDCF40D46121}
	Batch program=C:\PANalytical\Data Collector\Programs\Xcelerator batch.xrdmp, Identifier={35FAB0EB-D6DB-460E-9810-038470CBD570}
	MO 1
Measurement Date / Time:	6/16/2016 2:12:54 PM
Operator:	SEMCAL_XRD
Raw Data Origin:	XRD measurement (*.XRDML)
Scan Axis:	Gonio
Start Position [°2Th.]:	5.0084
End Position [°2Th.]:	69.9824
Step Size [°2Th.]:	0.0170
Scan Step Time [s]:	20.3200
Scan Type:	Continuous
PSD Mode:	Scanning
PSD Length [°2Th.]:	2.12
Offset [°2Th.]:	0.0000
Divergence Slit Type:	Fixed
Divergence Slit Size [°]:	0.2177
Specimen Length [mm]:	10.00
Measurement Temperature [°C]:	25.00
Anode Material:	Cu
K-Alpha1 [Å]:	1.54060
K-Alpha2 [Å]:	1.54443
K-Beta [Å]:	1.39225
K-A2 / K-A1 Ratio:	0.50000
Generator Settings:	40 mA, 45 kV
Diffractometer Type:	0000000011117966
Diffractometer Number:	0
Goniometer Radius [mm]:	240.00
Dist. Focus-Diverg. Slit [mm]:	100.00
Incident Beam Monochromator:	No
Spinning:	Yes

Document History

Insert Measurement:
- File name = "MO 1.xrdml"
- Modification time = "10/4/2017 4:29:12 PM"
- Modification editor = "SEMCAL_XRD"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "10/4/2017 4:29:12 PM"
- Modification editor = "SEMCAL_XRD"

Interpolate Step Size:
- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "10/4/2017 4:29:12 PM"
- Modification editor = "PANalytical"

Determine Background:
- Add to net scan = "Nothing"
- User defined intensity = "-5"
- Correction method = "Automatic"
- Bending factor = "2"
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "No"
- Granularity = "20"
- Modification time = "10/4/2017 1:21:36 PM"
- Modification editor = "SEMCAL_XRD"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.1"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "4/28/2017 4:58:53 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "61.0717"
- Modification time = "10/4/2017 4:32:03 PM"
- Modification editor = "SEMCAL_XRD"

Insert Peak:
- Peak position [°2Th.] = "64.2336"
- Modification time = "10/4/2017 4:32:08 PM"
- Modification editor = "SEMCAL_XRD"

Search & Match:
- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "Yes"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "50"
- Min. new lines / total lines = "60"
- Search depth = "10"
- Minimum new lines = "5"
- Minimum scale factor = "0.1"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "10/4/2017 4:33:09 PM"
- Modification editor = "SEMCAL_XRD"